{"id":17722,"date":"2015-04-01T12:00:55","date_gmt":"2015-04-01T09:00:55","guid":{"rendered":"http:\/\/balarisi.org\/?p=17722"},"modified":"2015-04-09T15:06:12","modified_gmt":"2015-04-09T12:06:12","slug":"elazig-yoresinde-satilan-suzme-ballarda-turev-spektrofotometri-ile-oksitetrasiklin-ve-sulfamezatin-tayini","status":"publish","type":"post","link":"https:\/\/www.beyazkovan.com\/?p=17722","title":{"rendered":"Elaz\u0131\u011f y\u00f6resinde sat\u0131lan s\u00fczme ballarda t\u00fcrev spektrofotometri ile oksitetrasiklin ve s\u00fclfamezatin tayini"},"content":{"rendered":"<p><strong>Meral Turabik<\/strong><br \/>\nY\u00fcksek Lisans Tezi, F\u0131rat \u00dcniversitesi \/ Fen Bilimleri Enstit\u00fcs\u00fc \/ Kimya M\u00fchendisli\u011fi Anabilim Dal\u0131, 1995, 75 s.<br \/>\nTEZ NO: <strong>45621<\/strong><br \/>\n<!--more--><span style=\"color: #ff6600;\"><a style=\"color: #ff6600;\" href=\"https:\/\/tez.yok.gov.tr\/UlusalTezMerkezi\/tarama.jsp\" target=\"_blank\">Sorgu Penceresine TEZ NO&#8217;yu yazarak Ayr\u0131nt\u0131l\u0131 Bilgi ve PDF d\u00f6k\u00fcmana ula\u015fmak i\u00e7in t\u0131klay\u0131n\u0131z <\/a><\/span><\/p>\n<p><strong>\u00d6ZET<br \/>\n<\/strong> Oksitetrasiklin (OTO, s\u00fclfamazatin (SM) ve kar\u0131\u015f\u0131mlar\u0131 t\u00fcrev spektroskopisi y\u00f6ntemiyle analizlenmi\u015ftir. pH= 4.8 asetat tamponuyla haz\u0131rlanan farkl\u0131 konsantrasyon ve oranlarda OTC ve SM i\u00e7eren sulu saf \u00e7\u00f6zeltilerde, spektrumun 2\u00b0 t\u00fcrevi kullan\u0131ld\u0131\u011f\u0131nda, absorbans hatalar\u0131 ve ila\u00e7lar\u0131n etkile\u015fimi elimine edilerek, 230.5 n\u0131n de OTC&#8217;nin 239.5 n\u0131n de S\u0130\u0130&#8217;in tayini yap\u0131lm\u0131\u015ft\u0131r.Kalibrasyon e\u011frileri 4-16 ppm OTC ve 2-12 ppm SM d\u00fczeylerine kadar lineerdir. Farkl\u0131 konsantrasyonl ardaki OTC ve SM ile farkl\u0131 OTC\/SM kar\u0131\u015f\u0131mlar\u0131 % 90-96 d\u00fczeylerinde geri kazan\u0131labilmektedir.\u000bBalda OTC ve SM analizi i\u00e7in al\u0131nacak optimum bal \u00f6rne\u011fi miktar\u0131 0.5 g. d\u0131r. Spektrum 2\u00b0 t\u00fcrevi 370 nm de OTC&#8217;nin, 1\u00b0 t\u00fcrev ve 252 nm&#8217;de S\u0130\u0130&#8217;in tayini, \u00f6n ay\u0131rma i\u015flemlerine gerek kalmadan yap\u0131labilmektedir. 8-20 ppm d\u00fczeylerinde bala eklenen ila\u00e7lar\u0131n geri kazan\u0131lma oranlan OTC i\u00e7in % 91-93 ve SM i\u00e7in % 94-98&#8217;dir. OTC + SM&#8217;i birlikte i\u00e7eren bal \u00f6rneklerinde OTC\/SM oran\u0131 1:1-3:1 aral\u0131\u011f\u0131nda., OTC geri kazanma oran\u0131 190-95., SM\/OTC oram 1:1-1:3 aral\u0131\u011f\u0131nda ise 195-96 d\u0131r. \u00d6zge\u00e7mi\u015fi bilinmeyen bal \u00f6rneklerinde standart ekleme y\u00f6ntemiyle spektrum 2* t\u00fcrevi 230.5 n\u0131n de OTC ve 1\u00b0 t\u00fcrev 254.6 n\u0131n de SM tayin edilebilmektedir.\u000b<strong>Anahtar Kelimeler: <\/strong> 0xytetracycline; derivative spectrophotometry; honey analysis; spectroscopy.; sulphamezathine<\/p>\n","protected":false},"excerpt":{"rendered":"<p>Meral Turabik Y\u00fcksek Lisans Tezi, F\u0131rat \u00dcniversitesi \/ Fen Bilimleri Enstit\u00fcs\u00fc \/ Kimya M\u00fchendisli\u011fi Anabilim Dal\u0131, 1995, 75 s. TEZ NO: 45621<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_bbp_topic_count":0,"_bbp_reply_count":0,"_bbp_total_topic_count":0,"_bbp_total_reply_count":0,"_bbp_voice_count":0,"_bbp_anonymous_reply_count":0,"_bbp_topic_count_hidden":0,"_bbp_reply_count_hidden":0,"_bbp_forum_subforum_count":0,"footnotes":""},"categories":[37],"tags":[],"class_list":["post-17722","post","type-post","status-publish","format-standard","","category-yuksek-lisans-tezleri","yazarlar-meral-turabik","anahtarkelimeler-antibiyotik-kalintisi","anahtarkelimeler-bal","anahtarkelimeler-bal-analizi","anahtarkelimeler-bal-ve-kalinti-sorunu","anahtarkelimeler-bal-ve-yoresel-arastirmalar","anahtarkelimeler-elazig","anahtarkelimeler-kalinti","anahtarkelimeler-kalinti-analizi","anahtarkelimeler-yoresel-arastirmalar"],"_links":{"self":[{"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=\/wp\/v2\/posts\/17722","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=17722"}],"version-history":[{"count":1,"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=\/wp\/v2\/posts\/17722\/revisions"}],"predecessor-version":[{"id":17723,"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=\/wp\/v2\/posts\/17722\/revisions\/17723"}],"wp:attachment":[{"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=17722"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=17722"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.beyazkovan.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=17722"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}